V. What are the drying methods of aerogel and their differences? Why is it said that aerogels prepared by ethanol supercritical drying have the most uniform nanoporous structure and the best thermal stability?
1. Drying Methods of Aerogels and Their Differences
Drying is the most critical step in aerogel fabrication. The goal is to remove solvents while preserving the 3D nanoporous network. Main methods include:
(1)Ambient Pressure Drying (APD)
· Low cost, but large shrinkage and uneven pore distribution result in degraded performance.
(2)Freeze Drying (FD)
· Removes solvent by sublimating ice; however, large pores or collapse may occur.
(3)Supercritical CO₂ Drying (CO₂-SCD)
· Mild conditions, decent pore retention, but requires multiple solvent exchanges and pore uniformity is limited.
(4)Supercritical Ethanol Drying (EtOH-SCD)
· Directly dries under ethanol supercritical conditions, eliminating capillary stress.
· Produces the most uniform nanopore distribution, high porosity, large surface area, and excellent thermal stability.
· Silica aerogels remain intact even at 500–1000℃.
In summary: Aerogels prepared by EtOH-SCD have the most uniform nanoporous structure and best thermal stability, making them the top choice for high-end applications.
2. IBIH is a global leader in using ethanol supercritical drying technology to mass-produce high-quality aerogels.
IBIH employs advanced EtOH-SCD technology with proprietary large-scale horizontal drying equipment.
Achieved industrial-scale production from lab to tens of thousands of metric square metres, with full intellectual property rights.
Performance Highlights:
· Porosity up to 85–99% with narrow pore size distribution.
· Thermal conductivity as low as 0.016 W/(m·K).
· Structural stability maintained at 500–1000℃
· Visible light transmittance >80%, suitable for translucent insulation.
· Excellent compressive resilience and long service life.
Overall Evaluation:
IBIH’s EtOH-SCD silica aerogels combine ultralow thermal conductivity, exceptional thermal stability, and optical transparency, representing the global top level. They are especially suited for high-end applications in energy-efficient buildings, new energy batteries, and aerospace.